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核磁共振光譜儀

Nuclear Magnetic Resonance Spectrometer

Instrument introduction:

Nuclear Magnetic Resonance (NMR) spectroscopy is a high-precision analytical technique that exploits the resonance phenomenon of atomic nuclei in a strong magnetic field under radiofrequency pulses to obtain detailed information on molecular structure and chemical environments. When nuclei with intrinsic spin (such as ¹H and ¹³C) are placed in a stable magnetic field and excited by radiofrequency irradiation, they generate detectable signals that, after Fourier transformation, yield NMR spectra. These spectra are used to elucidate molecular structures, functional groups, bonding relationships, and molecular dynamics. The instrument employs the JEOL JNM-ECZL series FT-NMR system (e.g., ECZ500 class), featuring high magnetic field stability and advanced digital radiofrequency control technology. It supports both one-dimensional and two-dimensional NMR experiments, including multinuclear measurements such as ¹H and ¹³C, as well as structural elucidation experiments such as COSY, HSQC, and HMBC. In addition, the system can be equipped with automatic sample changing and variable-temperature accessories to enhance analytical efficiency and experimental flexibility. Such NMR instruments are widely applied in organic synthesis, medicinal chemistry, materials science, and life science research, and are indispensable analytical tools for molecular structure determination and fundamental research.

Testing services:

500MHz Spectral Analysis
1-D spectra
2-D spectra (Please contact the instrument operator.)
V-T NMR (Please contact the instrument operator.)

Instructions for submitting for testing:

  • For external testing services, please contact the administrator and the instrument operator to confirm the scope of services and to make an appointment.
  • Please ensure that the sample submission form is completed accurately and submit it together with the samples to the Department of Chemistry, National Dong Hwa University. Incomplete forms may result in delays in sample processing or collection.
  • Users submitting samples for analysis may place the samples in sample vials and mail them to our department. Test tubes and commonly used solvents are available, and sample preparation can be performed on behalf of the user.
  • Test only liquid samples. Use a solvent containing deuterium (D). Prepare samples weighing about 10–50 mg, ensuring they are fully dissolved without any suspended solids.
  • For valuable samples, the submitter must prepare the sample independently. Contact the administrator beforehand to reserve the sample, and ensure that the original sample is retrieved by the submitter.
  • Users performing self-testing should prepare NMR tubes at least 15 cm long, without bending and with undamaged openings. Fill the sample to a height of 4–5 cm, then seal the tube opening to avoid contamination and evaporation.
  • To avoid damaging the instrument coil and the insert glass between the coil and the NMR sample tube, use certified NMR tubes, e.g., types 507 or 528.
  • Reserve time in advance for special samples or extended testing sessions, including those conducted during holidays.
  • The client shall not use the test results for commercial advertising, evidence in legal proceedings, or other purposes without the consent of the Center. Violators will be prosecuted by the Center in accordance with the law. If the center's reputation is damaged due to the client's improper use of test reports, the center will demand compensation for damages in accordance with the law.

Service items and charging standards:

NMR 500 MHz Sample Processing Fee (per hour, assisted measurement)

a.Scheduled Reservation – Assisted Measurement

1000/hr

b.Non-scheduled Reservation – Assisted Measurement

1500/hr

c.Scheduled Reservation – Self Measurement

N/A

c.Non-scheduled Reservation – Self Measurement

N/A

NMR 500 MHz 1D and 2D Spectra (per hour)

a.Scheduled Reservation – Assisted Measurement

400/hr

b.Non-scheduled Reservation – Assisted Measurement

800/hr

c.Scheduled Reservation – Self Measurement

60/hr

c.Non-scheduled Reservation – Self Measurement

120/hr

NMR 500 MHz Extended Holiday Experiment (12 hours)

a.Scheduled Reservation – Assisted Measurement

3000

b.Non-scheduled Reservation – Assisted Measurement

6000

c.Scheduled Reservation – Self Measurement

600

c.Non-scheduled Reservation – Self Measurement

1200

contact person :

Responsible professor: Kuo-Ting Chen
Tel: 03-8903603
e-mail: ktchen26@gms.ndhu.edu.tw

Instrument Manager: CHENG,LI-CHIN
e-mail: 411112003@gms.ndhu.edu.tw